Determination of aromatic compounds in Malaysian commercialized petrol using solid phase micro extraction (SPME) coupled to gas chromatography mass spectrometry detector (GC-MSD) / Mohamad Rosdi Muhammad Razali

Muhammad Razali, Mohamad Rosdi (2012) Determination of aromatic compounds in Malaysian commercialized petrol using solid phase micro extraction (SPME) coupled to gas chromatography mass spectrometry detector (GC-MSD) / Mohamad Rosdi Muhammad Razali. Degree thesis, Universiti Teknologi MARA (UiTM).

Abstract

A method for the identification of aromatic compounds in different varieties of petrol by using solid phase microextraction (SPME) and gas chromatography-mass spectrometry detector (GC-MS) was developed. SPME fiber coated with polydimethylsiloxane (PDMS) was used in this study. The effects of important SPME parameters such as desorption time, extraction time and extraction temperature on the amount of compounds extracted were studied. Optimum conditions for SPME were 40°C for extraction temperature, 10 minutes for extraction time and 100 seconds for desorption time. Using the optimized conditions, aromatic compounds in different samples were determined and the benzene concentration in the samples were compared. It was found that petrol XI has the highest benzene concentration compared to other petrol samples.

Metadata

Item Type:	Thesis (Degree)
Creators:	Creators Email / ID Num. Muhammad Razali, Mohamad Rosdi UNSPECIFIED
Contributors:	Contribution Name Email / ID Num. Thesis advisor Abdullah Munir, Zuraidah UNSPECIFIED
Subjects:	Q Science > QC Physics > Optics. Light > Spectroscopy Q Science > QD Chemistry > Analytical chemistry
Divisions:	Universiti Teknologi MARA, Shah Alam > Faculty of Applied Sciences
Programme:	Bachelor of Science (Hons.) Chemistry
Keywords:	Detector, gas, aromatic
Date:	July 2012
URI:	https://ir.uitm.edu.my/id/eprint/74340