Morphological, structural and optical properties of ZnO nanowires: The effect of growth time / Nurul Zulaikha Mohd Zamri ... [et al.]

Mohd Zamri, Nurul Zulaikha and Malek, Mohd Firdaus and Mohammad, Maryam and Bakri, Mohd Dzulfiqar and Rostan, Nur Fairuz and Khairul Azhar, Nurfatini Atiqrah and Mamat, Mohamad Hafiz and Shamsudin, Muhammad Salleh and Mahmood, Mohamad Rusop (2023) Morphological, structural and optical properties of ZnO nanowires: The effect of growth time / Nurul Zulaikha Mohd Zamri ... [et al.]. Malaysian Journal of Chemical Engineering and Technology (MJCET), 6 (2): 5. pp. 81-87. ISSN 2682-8588
Identification Number (DOI): 10.24191/mjcet.v6i2.21842
Abstract

Zinc oxide (ZnO) nanostructures (NSs) such as nanowires (NWs), nanorods, nanobelts, nanotubes, and nanonails have received a lot of attention in recent years due to their exceptional chemical and physical characteristics and wide range of potential uses. Researchers have investigated its possible uses in optoelectronic devices, field emitters, solar cells, sensors, and transparent electrodes due to its special features. This work is focused on a new method for the synthesis of ZnO NSs, particularly ZnO NWs, via microwave-assisted ultrasonic technique, with the advantages of low cost and the potential for large scale. The samples were evaluated with respect to the structural, morphological, and optical properties using various methods, such as field-emission scanning electron microscopy, X-ray diffraction, and UV-Vis spectroscopy. The reaction occurs in only 60 minutes with minimal energy expenditure. ZnO NWs produced at 600 W had diameters ranging between 33.53 and 41.81 nm and lengths that varied between 1.84 and 2.1 μm, were totally crystalline, and showed preferential growth in the (002) direction, which presented a hexagonal wurtzite structure.

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