Characterization of agarwood incense using gas chromatography – mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail … [et al.]

Ismail, Nurlaila and Ibrahim, Mastura and Zareen, Seema and Rahiman, Mohd Hezri Fazalul and Tajuddin, Saiful Nizam and Taib, Mohd Nasir (2015) Characterization of agarwood incense using gas chromatography – mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail … [et al.]. Scientific Research Journal, 12 (2). pp. 68-81. ISSN 1675-7009

Official URL: https://srj.uitm.edu.my/

Abstract

This paper presents the application of Solid Phase Micro Extraction (SPME) coupled with Gas Chromatography-Mass Spectrometry (GC-MS) and Gas Chromatography-Flame Ionization Detector (GC-FID) to characterize agarwood incense. The work involved three types of SPME fibres at 30 minutes sampling time. The fibres are 50/30 jum divinylbenzene-carboxenpolydimethysiloxane (DVB-CAR-PDMS), 65 jum polydi methylsiloxanedivinylbenzene (PDMS-DVB) and 85 jum carboxen-polydimethyl siloxane (CAR-PDMS). The results showed that among many compounds extracted by GC-MS coupled with SPME, six compounds were found significantly presence in high quality agarwood incense due to their high percentage area (%). They are (5-maaliene, ᵝ-elemol, ᵝ-selinene, 10-epi-y-eudesmol, agarospirol and caryophellene oxide. The finding offers a new approach for establishing the volatile profile of agarwood incense components which is beneficial for agarwood grading and discrimination.

Metadata

Item Type: Article
Creators:
Creators
Email / ID Num.
Ismail, Nurlaila
UNSPECIFIED
Ibrahim, Mastura
UNSPECIFIED
Zareen, Seema
UNSPECIFIED
Rahiman, Mohd Hezri Fazalul
UNSPECIFIED
Tajuddin, Saiful Nizam
UNSPECIFIED
Taib, Mohd Nasir
UNSPECIFIED
Subjects: T Technology > TP Chemical technology > Chemical engineering > Special processes and operations > Extraction
Divisions: Universiti Teknologi MARA, Shah Alam > Research Management Centre (RMC)
Journal or Publication Title: Scientific Research Journal
UiTM Journal Collections: UiTM Journal > Scientific Research Journal (SRJ)
ISSN: 1675-7009
Volume: 12
Number: 2
Page Range: pp. 68-81
Keywords: Agarwood incense, high quality, GC-MS coupled with SPME, GC-FID
Date: 2015
URI: https://ir.uitm.edu.my/id/eprint/16086
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