Synthesis and decarboxylation Of 2-(4-Methoxylphenyl)-1-Methyl-4,5-Dioxo-Pyrollidine-3-Carboxylic Acid Ethyl Ester / Islaili Ulfah Yaakob

Yaakob, Islaili Ulfah (2009) Synthesis and decarboxylation Of 2-(4-Methoxylphenyl)-1-Methyl-4,5-Dioxo-Pyrollidine-3-Carboxylic Acid Ethyl Ester / Islaili Ulfah Yaakob. Student Project. Faculty of Applied Sciences, UiTM Shah Alam. (Unpublished)

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Abstract

The main focus of this experiment was synthesizing 2,3-dioxopyrrolidine for the first part. There were three main reagents to achieve the first part of this experiment. The reagents were diethyl oxalate, methyl amine and aldehyde groups. The two different aldehyde groups used were anisaldehyde and benzaldehyde. The structures of the 2,3-dioxopyrrolidine were determined using NMR. The second part of this experiment is decarboxylation. Each product from the first part underwent reflux for 2 hours in 10% HCl. The mixture obtained from decarboxylation was extracted with dicholomethane and ethyl acetate. The mixture then evaporated under reduced pressure.

Item Type: Monograph (Student Project)
Creators:
CreatorsEmail
Yaakob, Islaili UlfahUNSPECIFIED
Subjects: Q Science > QD Chemistry
Divisions: Faculty of Applied Sciences
Item ID: 495
Last Modified: 16 Oct 2018 07:07
Depositing User: Staf Pendigitalan 1
URI: http://ir.uitm.edu.my/id/eprint/495

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