Synthesis and characterization of zinc-layered 2, 4, 5 trichlorophenoxybutyric acid under aqueous condition / Nur Hani Ab Rahman

Ab Rahman, Nur Hani (2016) Synthesis and characterization of zinc-layered 2, 4, 5 trichlorophenoxybutyric acid under aqueous condition / Nur Hani Ab Rahman. Student Project. Faculty of Applied Sciences, Kuala Pilah, Negeri Sembilan. (Unpublished)

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Abstract

The synthesis of zinc-layered 2, 4, 5-triclorophenoxybutyric acid (ZTBA) and the characterization of the nanohybrid compound by using powder x-ray diffraction (PXRD), Fourier Transform Infrared (FTIR), Thermogravimetric and Derivative Thermogravimetric Analysis (TGA/DTG) and Elemental Analysis (CHNS) has been developed. The synthesis of the ZTBA nanohybrid compound was successfully prepared by using anion-exchange method. The pure phase and well-ordered zinc-layered 2, 4, 5-trichlorophenoxybutyric acid was synthesized at 0.1 M 2, 4, 5-trichlorophenoxybutyric acid (TBA) and with a basal spacing of 13.0 Å. The FTIR spectra show resemblance of TBA with ZnO absorption characteristics. The percentage loading of guest anions, TBA in the zinc layered hydroxide was calculated to be about 51.92 % .The total weight loss by using TGA / DTG is calculated to be at about 63.5 % in the range of 90 - 1000⁰C.

Item Type: Monograph (Student Project)
Creators:
CreatorsEmail
Ab Rahman, Nur HaniUNSPECIFIED
Subjects: Q Science > QD Chemistry
Q Science > QD Chemistry > Metal complexes. Layered double hydroxides
Divisions: Universiti Teknologi MARA, Negeri Sembilan > Kuala Pilah Campus > Faculty of Applied Sciences (N)
Item ID: 24267
Uncontrolled Keywords: Synthesis and characterization, of zinc-layered 2, 4, 5 trichlorophenoxybutyric acid, under aqueous condition, UiTM Negeri Sembilan
Last Modified: 17 May 2019 07:39
Depositing User: Perpustakaan Tun Abdul Razak UiTM Cawangan Negeri Sembilan
URI: http://ir.uitm.edu.my/id/eprint/24267

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