Characterization of agarwood incense using gas chromatography – mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail … [et al.]

Ismail, Nurlaila and Ibrahim, Mastura and Zareen, Seema and Rahiman, Mohd Hezri Fazalul and Tajuddin, Saiful Nizam and Taib, Mohd Nasir (2015) Characterization of agarwood incense using gas chromatography – mass spectrometry (GC-MS) coupled with solid phase micro extraction (SPME) and gas chromatography - flame ionization detector (GC-FID) / Nurlaila Ismail … [et al.]. Scientific Research Journal, 12 (2). pp. 68-81. ISSN 1675-7009

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Abstract

This paper presents the application of Solid Phase Micro Extraction (SPME) coupled with Gas Chromatography-Mass Spectrometry (GC-MS) and Gas Chromatography-Flame Ionization Detector (GC-FID) to characterize agarwood incense. The work involved three types of SPME fibres at 30 minutes sampling time. The fibres are 50/30 jum divinylbenzene-carboxenpolydimethysiloxane (DVB-CAR-PDMS), 65 jum polydi methylsiloxanedivinylbenzene (PDMS-DVB) and 85 jum carboxen-polydimethyl siloxane (CAR-PDMS). The results showed that among many compounds extracted by GC-MS coupled with SPME, six compounds were found significantly presence in high quality agarwood incense due to their high percentage area (%). They are (5-maaliene, ᵝ-elemol, ᵝ-selinene, 10-epi-y-eudesmol, agarospirol and caryophellene oxide. The finding offers a new approach for establishing the volatile profile of agarwood incense components which is beneficial for agarwood grading and discrimination.

Item Type: Article
Creators:
CreatorsEmail
Ismail, NurlailaUNSPECIFIED
Ibrahim, MasturaUNSPECIFIED
Zareen, SeemaUNSPECIFIED
Rahiman, Mohd Hezri FazalulUNSPECIFIED
Tajuddin, Saiful NizamUNSPECIFIED
Taib, Mohd NasirUNSPECIFIED
Subjects: T Technology > TP Chemical technology > Chemical engineering > Special processes and operations > Extraction
Divisions: Institute of Research Management and Innovation (IRMI)
Journal or Publication Title: Scientific Research Journal
ISSN: 1675-7009
Volume: 12
Number: 2
Page Range: pp. 68-81
Item ID: 16086
Uncontrolled Keywords: Agarwood incense, high quality, GC-MS coupled with SPME, GC-FID
Last Modified: 02 Feb 2017 07:10
Depositing User: Staf Pendigitalan 5
URI: http://ir.uitm.edu.my/id/eprint/16086

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