Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin

Che Soh, Siti Kamilah and Jusoh, Siti Aminah and Shamsuddin, Mustaffa (2014) Synthesis and physicochemical analysis of Polystyrene-Anchored Pd(II) metal complex / Siti Kamilah Che Soh, Siti Aminah Jusoh and Mustaffa Shamsuddin. Scientific Research Journal, 11 (2). pp. 1-10. ISSN 1675-7009

Abstract

A polystyrene (PS)-anchored Pd(II) metal complex was synthesized on cross-linked polymer by heating a mixture of chlorometylated polystyrene with phenyldithiocarbazate and carbon disulfide in the presence of potassium hydroxide (KOH) in dimethylformamide (DMF). The reaction mixture was heated at 80 °C to form the corresponding phenyldithiocarbazate-functionalized polymer. Then, it was treated with bis(benzonitrile)palladium(II) chloride. The properties of dark colored polymer, impregnated with the metal complex was then characterized by various spectroscopic technique such as Fourier Transform Infrared (FTIR), Scanning Electron Microscopy/Energy Dispersive X-ray (SEM/EDX), CHNS elemental analysis, BET surface area, X-ray Diffraction (XRD), Thermogravimetric (TGA) and Inductively Coupled Plasma-Optical Emission (ICP-OES) spectroscopy.

Download

[img] Text
AJ_SITI KAMILAH CHE SOH SRJ 14 1.pdf

Download (439kB)

Metadata

Item Type: Article
Creators:
CreatorsID Num.
Che Soh, Siti Kamilahsitikamilah@umt.edu.my
Jusoh, Siti AminahUNSPECIFIED
Shamsuddin, MustaffaUNSPECIFIED
Subjects: Q Science > QD Chemistry > Inorganic chemistry > Palladium
T Technology > TP Chemical technology > Polystyrene
Divisions: Research Management Institute (RMI)
Journal or Publication Title: Scientific Research Journal
ISSN: 1675-7009
Volume: 11
Number: 2
Page Range: pp. 1-10
Item ID: 12430
Uncontrolled Keywords: Polystyrene; Palladium; Catalyst
URI: http://ir.uitm.edu.my/id/eprint/12430

Actions (login required)

View Item View Item

Downloads

Downloads per month over past year